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N-(4-Chloro-3-nitrophenyl)acetamide
- Name: N-(4-Chloro-3-nitrophenyl)acetamide
- CAS: 5540-60-3
- Purity: 99%
Details
N-(4-Chloro-3-nitrophenyl)acetamide Good Manufacturer supply High Quality 5540-60-3
- Molecular Formula: C8H7 Cl N2 O3
- Molecular Weight: 214.608
- Vapor Pressure: 1.99E-18mmHg at 25°C
- Melting Point: 125-129 ºC
- Refractive Index: 1.778
- Boiling Point: 404.1°Cat760mmHg
- PKA: 13.33±0.70(Predicted)
- Flash Point: 198.2°C
- PSA： 88.91000
- Density: 1.466g/cm3
- LogP: 2.49950
N-(4-Chloro-3-nitrophenyl)acetamide(Cas 5540-60-3) Usage
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Synthesis Reference(s) |
The Journal of Organic Chemistry, 26, p. 1418, 1961 DOI: 10.1021/jo01064a022 |
InChI:InChI=1/C19H11NO5/c21-15-9-11(7-8-12(15)19(24)25)20-17(22)13-5-1-3-10-4-2-6-14(16(10)13)18(20)23/h1-9,21H,(H,24,25)
5540-60-3 Relevant articles
Pyridine compound, preparation method and application thereof, and pharmaceutical composition
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5540-60-3 Process route
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C8 H7 ClN2 O3
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-
5540-60-3
N-(4-chloro-3-nitrophenyl)acetamide
| Conditions | Yield |
|---|---|
|
With
2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide;
In
tetrahydrofuran; ethyl acetate;
at 70 ℃;
Inert atmosphere;
|
95%
|
-
-
635-22-3
4-Chloro-3-nitroaniline
-
-
108-24-7
acetic anhydride
-
-
5540-60-3
N-(4-chloro-3-nitrophenyl)acetamide
| Conditions | Yield |
|---|---|
|
With
nickel dichloride;
at 20 ℃;
for 0.166667h;
Neat (no solvent);
|
95%
|
|
With
sulfuric acid;
for 2h;
Heating;
|
81%
|
|
In
dichloromethane;
at 20 ℃;
for 2h;
|
80%
|
|
With
benzene;
|
|
|
With
sulfuric acid;
|
|
|
Inert atmosphere;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 40 - 50 ℃;
for 2h;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 40 - 50 ℃;
for 2h;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 40 - 50 ℃;
for 2.25h;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 10 - 20 ℃;
for 1.08333h;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 40 - 50 ℃;
for 2.25h;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 40 - 50 ℃;
for 2h;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 40 - 50 ℃;
for 2h;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 40 - 50 ℃;
for 2h;
|
|
|
In
1-methyl-pyrrolidin-2-one;
at 40 - 50 ℃;
for 2h;
|
5540-60-3 Upstream products
-
635-22-3
4-Chloro-3-nitroaniline
-
108-24-7
acetic anhydride
-
64-19-7
acetic acid
-
539-03-7
N-(4-chlorophenyl)acetamide
5540-60-3 Downstream products
-
74804-14-1
bis(4-acetylamino-2-nitrophenyl) disulphide
-
5367-35-1
N4 -Acetyl-N1 ,N1 -dimethyl-2-nitro-p-phenylendiamin
-
51867-83-5
1-amino-3-acetylamino-6-chloro-benzene
-
76209-01-3
4-acetylamino-2-nitrobenzenethiol
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